avatar
n*l
1
how dangerous it is to use sodium azide on 10 gram scale?
I need to transform an OH to a NH2 group and do not want to do the mess
workup of Mitsunobu reaction.
avatar
q*u
2
As long as the rest of your molecule is not a short chain, go ahead for 10
grams, Even 50 grams or 100 grams.
avatar
J*e
3
看你底物有几个炭,超过4个应该没问题。

【在 n***l 的大作中提到】
: how dangerous it is to use sodium azide on 10 gram scale?
: I need to transform an OH to a NH2 group and do not want to do the mess
: workup of Mitsunobu reaction.

avatar
n*1
4
Why not Gabriel?
avatar
M*d
5
做过N3-(CH2)3-N3,scale up没有问题……

【在 J**e 的大作中提到】
: 看你底物有几个炭,超过4个应该没问题。
avatar
n*l
6
Thanks, the molecule has 7 carbons.
One more question, is it ok to handle sodium azide with a metal spatula?
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