I cannot input chinese now, I saw the thread below discussing how to remove the residual solvent. http://www.mitbbs.com/article_t1/Chemistry/31280475_0_2.html I have a silmiar problem, and the solvent is encapuslated inside polymer. Here is what I did: A polymer (Tg ~ 270C) with 1% N-methyl pyrrolidone (NMP) solvent residue. This polymer can dissolve in THF, but not in water, methanol and acetone. We tried purification of this polymer by dissolving it in THF, then precipitated the solution in an