sodium azide - 未名空间MITBBS历史存档

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sodium azide

sodium azide# Chemistry - 化学

n*l2013-05-09 07:05

1 楼

how dangerous it is to use sodium azide on 10 gram scale?
I need to transform an OH to a NH2 group and do not want to do the mess
workup of Mitsunobu reaction.

q*u2013-05-09 07:05

2 楼

As long as the rest of your molecule is not a short chain, go ahead for 10
grams, Even 50 grams or 100 grams.

J*e2013-05-09 07:05

3 楼

看你底物有几个炭，超过4个应该没问题。

【在 n***l 的大作中提到】

: how dangerous it is to use sodium azide on 10 gram scale?
: I need to transform an OH to a NH2 group and do not want to do the mess
: workup of Mitsunobu reaction.